Guia docente 2016_17
Facultade de Química
Grao en Química
 Subjects
  Chemistry, physics and biology: Integrated laboratory I
   Contents
Topic Sub-topic
1) Norms of hygiene and security in the laboratory (1 session ).
2) basic Concepts of the calculation of errors in the measures: I handle of the calibrate and analysis of distribution of populations (1 session).
3) Recognition and utilisation of the basic material of laboratory. Design of a fascicle of laboratory (1 session ).
4) Determination of densities of liquids and solid (1 session).
5) Preparation of dissolutions (2 sessions):
to) From a solid solute (exact and approximate concentration).
*b) From a liquid solute (*Ej.: *HCl, *H2UNDER4, etc.).
*c) Prepare dissolutions diluted of the ready previously.
6) Measure of the superficial tension (1 session).
7) Measure of the *viscosidad (1 session).
8) Establishment of a chemical equation: stoichiometry (1 session).
9) Separation of the components of a mix by means of sublimation and leak (1 session).
10) Reactions of precipitation (1 session).
11) Purification of liquids: distillation (1 session).


12) Isolation of organic compounds: liquid extraction-liquid. (1 session).
13) Heat of reaction. (1 session).
14) Purification of solids: crystallisation. Measure of melting-points. (1 session).
15) Study of the chemical balance. Principle of Him *Chatelier (1 session):
to) Effect of the temperature.
*b) Effect of the concentration.
16) specific Heats of liquids and solid (1 session).
17) Extraction of present lipids in the *yema of egg. Methods of extraction and identification of the distinct types of lipids. Methods of chromatography in fine layer of lipids (*CCF) (1 session).
18) sour Volumetries-basic (2 sessions):
to) Assessment of hydroxide of sodium with hydrogen *ftalato of potassium.
*b) Assessment of acid *clorhídrico with the hydroxide of ready sodium in (to).
19) Isolation of nucleic acids. Method of extraction and identification of nucleic acids. Methods of colorimetric reaction (1 session).
20) Determination of the concentration of proteins in liver of rat. Realisation of a straight pattern (1 session).
21) Volumetries *redox (2 sessions):
to) Assessment of *oxalato of sodium with *permanganato of potassium.
*b) Determination of the concentration of a dissolution of *hipoclorito by means of assessment with *tiosulfato.
22) Isolation of glycogen. Extraction by means of precipitation and extraction with alcohol (1 session).
23) Determination of the concentration of glucose. Specific chemical methods colorimetric (1 session).
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